ELABORATION OF MASSIVE SILICA XEROGELS BY DEACIDIFICATION AND DRYING CONTROL

  • COSTILLE BENJAMIN
    Université de Limoges, SPCTS, UMR CNRS 7315, 12 rue Atlantis 87068 Limoges Cedex, France
  • BENROKIA SARAH
    Université de Limoges, SPCTS, UMR CNRS 7315, 12 rue Atlantis 87068 Limoges Cedex, France
  • THUNE ELSA
    Université de Limoges, SPCTS, UMR CNRS 7315, 12 rue Atlantis 87068 Limoges Cedex, France
  • GUINEBRETIERE RENE
    Université de Limoges, SPCTS, UMR CNRS 7315, 12 rue Atlantis 87068 Limoges Cedex, France

Abstract

In this article, the goal is to deacidify silica gels containing a large amount of hydrochloric acid necessary for the synthesis of mixed gels. A washing step is added to the gel preparation protocol, in order to remove a certain amount of acid and also to improve the drying, promoting non-cracked bulk gels. The results are promising, which allows to transpose this process to the elaboration of mixed gels.

Cuvinte cheie

sol-gel bulk xerogel washing deacidification drying